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Beilstein J. Org. Chem. 2021, 17, 2095–2101, doi:10.3762/bjoc.17.136
Graphical Abstract
Scheme 1: Schematic representation of the self-initiated photografting and photopolymerization (SIPGP) of 2-h...
Figure 1: A) Graph showing change in the static contact angle with time on a pristine PCL scaffold with a 500...
Figure 2: A) Optical photograph of an SIPGP-coated sample. B) 3D topography reconstruction of the SIPGP-coate...
Figure 3: A) SEM image of pristine, uncoated PCL MEW scaffolds with a hatch spacing of 150 µm × 200 µm and in...
Beilstein J. Org. Chem. 2016, 12, 1127–1135, doi:10.3762/bjoc.12.109
Figure 1: Structure of squalenic acid-d6, gemcitabine and GemSQ-d6 conjugate.
Scheme 1: Retrosynthetic route to SQCO2H-d6 (1) and synthetic routes for the preparation of dialdehyde 5 and ...
Scheme 2: Implementation of the deuterated isopropylidene end-group by the Shapiro reaction of trisylhydrazon...
Scheme 3: Attempted synthesis of 1 via the protection of the aldehyde 10 as a 5,5-dimethyl-1,3-dioxane.
Scheme 4: Synthesis of squalenic acid-d6 1 and conjugation to gemcitabine.
Figure 2: A) Sketch depicting the procedure of preparing the NAs. B) Single Raman spectra of GemSQ-d6 NAs, Ge...